Here is my first attempt at growing some diamonds. This pic was just after I released the pressure. It is finishing off in vac chamber. Now. Going to be a good night!!!
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What’s this process?
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This was 400 wet grams fresh material. Ran with n-Tane with dewaxing jacket (Didn’t get material and solvent cold enough) which left some wax and lipids causing darker color.
I recovered n-tane at 90df. I put about 1 quart of solvent filled trichome into a mason jar and placed in dry ice slurry for 2 days with lid loose. The mixture at 1/3 left I capped tight and placed in oven at 85df for 10 days. After raised temp to 120df with cap off and -20hg vacuum for 12 hours and wallah.
Lessons learned on this one
Get material and solvent much much colder. I plan to place in dry lcd slurry overnight next time to help with color.
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